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2 edition of Determination of hydrocarbons in aqueous effluents from the oil industry by infrared analysis. found in the catalog.

Determination of hydrocarbons in aqueous effluents from the oil industry by infrared analysis.

Concawe. Special Task Force on Guidelines on Tests and Standardised Methods.

Determination of hydrocarbons in aqueous effluents from the oil industry by infrared analysis.

by Concawe. Special Task Force on Guidelines on Tests and Standardised Methods.

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  • 23 Currently reading

Published by CONCAWE .
Written in English


Edition Notes

SeriesReport no 1/84
ID Numbers
Open LibraryOL20698990M

Created Date: 10/25/ PM. Near-infrared spectroscopy, chemicals, process monitoring, chemical reaction, moisture determination, hydrocarbon, acid, resin, solvent. No. 9: Monitoring water in Summary This Application Bulletin shows the examples of NIR applications and the feasibility studies using NIRSystems in the chemical industry. It includes qualitative and quantitative.

  1. Introduction. In order to interpret, evaluate the risk and make decisions about potential hazardous effects of petroleum hydrocarbons and ensure the appropriate protection of the environment, it is very important to have a sound understanding of the toxicology, analytical science, environmental fate and behaviour, risk and technological implications of petroleum hydrocarbons. A high-performance liquid chromatography gradient scheme has been used to separate the aromatic hydrocarbons in the aqueous effluents of a coal gasification process. Samples of raw water, activated sludge, and activated sludge plus carbon-treated effluents were evaluated.

This test method covers the determination of fluorocarbon-extractable substances as an estimation of the combined oil and grease and the petroleum hydrocarbon contents of a sample of water or waste water in the range from to mg/L. It is the user's responsibility to assume the validity of the standard for untested types of water.   The Collection and Infrared Analysis of Low Molecular Weight Hydrocarbons from Combustion Effluents. American Industrial Hygiene Association Journal , 20 (5), DOI: /


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Determination of hydrocarbons in aqueous effluents from the oil industry by infrared analysis by Concawe. Special Task Force on Guidelines on Tests and Standardised Methods. Download PDF EPUB FB2

Precautions No known solvent will dissolve effectively only oil and grease. Solvent removal results in the loss of short chain hydrocarbon and simple aromatic compound by volatilisation, and heavier residual of some effluents may contain significant portion of material that are not extracted with the solvent.

CONCAWE,“Determination of Hydrocarbons in Aqueous Effluents from the Oil Industry by Infrared Analysis”, prepared by CONCAWE’s Special Task Force on Guidelines on Tests and Standard Methods (). Google ScholarCited by: 4. Several methods of extraction and analytical determination for total petroleum hydrocarbons (TPHCs) in aqueous and solid samples are reviewed.

Infrared spectroscopy is one of the efficient methods that are being replaced today pursuant to getting rid of some halogenated solvents classified as ozone-depleting substances. The gravimetric method which uses n Cited by:   A new robust method for determination of hydrocarbons in water without use of Freon [21 CONCAWE, Determination of Hydrocarbons in Aqueous Effluents from the Oil Industry by Infrared Analysis, Prepared by CONCAWE's Special Task Force on Guidelines on Tests and Standard Methods () [3] G.F.

Oldham, Methods of Analysis and Sampling of Oil Cited by: 4. This test method covers the determination of total oil and grease (TOG) and total petroleum hydrocarbons (TPH) in water and waste water that are extractable by this test method from an acidified sample with a cyclic aliphatic hydrocarbon (for example cyclohexane, cyclopentane) and measured by IR absorption in the region from cm-1 to cm-1 ( μm to.

Determination of Hydrocarbon Residues in Water RATI-IER J. () Determination of oil in refinery effluent waters. Analyt. Chem. 30, ROSEN A. and MIDDI~rON F.

() Identification of petroleum refinery wastes in surface waters. Analyt. Chem. 27, SHEET J. () Determination of volatile oil in effluents. It is important to the oil refining industry to obtain accurate and reliable data on the levels of hydrocarbons in aqueous discharges.

However, considerable difficulties are presented in. Ecological monitoring of aqueous effluents from petroleum refineries 8/82 Determination of hydrocarbons in aqueous effluents from the oil industry by infrared analysis 1/84 Collection and disposal of used lubricating oil 5/96 European oil industry guideline for risk-based assessment of contaminated sites (revised) 3/   Oil and Grease Analysis Oil and grease includes fats, oils, waxes, and other related constituents found in water, generally wastewater.

If these compounds are not removed before discharge of treated wastewater, oil and grease can interfere with biological life in surface waters and create unsightly films. Fats and oils are contributed to domestic wastewater in.

transformations of petroleum hydrocarbons in the environment. The methods generally employed to measure the TOG in the oil industry are gravimetry and infrared spectrometry [6, 7].

Gravimetric methods, such as Method and Standard Method B from the U.S. Environmental Protection Agency (EPA), involve liquid-liquid extraction. infrared and mass spectrometric, the latter types being necessary to achieve speciation of Formerly, the idea of total hydrocarbon determination in soil was seen as providing a satisfactory tool for assessing contaminated sites.

Modern hydrocarbon type. Shale oil retorting plants provide another source of hydrocarbon. Rotteri, S; H Boertzler; J Dubreuil et al, Determination of hydrocaronbs in aqueous effluents from the oil industry by infrared analysis.

Concawe. A direct aqueous supercritical fluid extraction (SFE) system was developed which can be directly interfaced to an infrared spectrometer for the determination of oil in water.

The technique is designed to provide an environmentally clean, automated alternative to established IR methods for oil in water analysis. EPA promulgated the Oil and Gas Extraction Effluent Guidelines and Standards (40 CFR Part ) inand amended the regulations in, and The regulations cover wastewater discharges from field exploration, drilling, production, well treatment and well completion activities.

Common oil in water analysis reference methods include infrared, gravimetric and GC-FID based, each has its own advantages and disadvantages. To get a good oil in water result, in addition to having a good analysis method, sampling and sample handling is equally important, as measurement can only produce a result as good as the sample can provide.

hydrocarbons (alkenes), and 35% aromatic hydrocarbons (including alkylbenzenes and 2- 3-ring aromatics) (Air Force ). Fuel oil #2 contains less than 5% polycyclic aromatic hydrocarbons (IARC b). The typical hydrocarbon composition of fuel oil #2 is presented in Table Eb (Appendix E).

Fuel Oil #6. erated by the sugarcane industry and the contamination of water produced by the petroleum industry (Branda˜o et al. Based on these aspects, the main objective and contri-bution of this work is to purpose a new process for treat-ment of contamination of aqueous sources by hydrocarbons from petroleum, using sugarcane bagasse as bioadsorbent.

Polycyclic aromatic hydrocarbons (PAHs) are major organic pollutants in the environment, which are toxic to humans and biota, given their carcinogenic, mutagenic and teratogenic nature.

In this chapter, we carried out an overview of the sources and toxicity of PAHs, their common analytical methods of determination in the water and sediment samples, and.

Determination of hydrocarbons in aqueous effluents from the oil industry by infrared analysis 1/84 Collection and disposal of used lubricating oil 5/96 European oil industry guideline for risk-based assessment of contaminated sites (revised) 3/03 A guide for reduction and disposal of waste from oil refineries and.

Oil analysis. Selected pages. Title Page. Table of Contents. Contents. Introduction. 3: D Test Method for Hydrocarbon Types Analysis of GasOil Saturates Fractions by High Ionizing. D Test Method for Determination of Carbonyls in C4 Hydrocarbons.

/5(2). 4 Measurement of Dispersed Oil in Produced Water Using Infrared Analysis Method – (and other samples containing hydrocarbons) in order to enable industry to comply This method is not to be used for the determination of oil in other discharges under OPPC, e.g.

oil on sand, drains discharges, etc.One example is the use of tetrachloroethylene as a replacement for carbon tetrachloride in oil and grease analysis by infrared spectroscopy.

hydrocarbons determination from water consist in.in the analysis of petroleum hydrocarbons in the en viron- m e n t[ ]. es a m p l em u s tb ec o l l e c t e dw i t h o u tc o n t a m i n a - tion and must be wholly representative of the.